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Thermogravimetric Analysis (TGA)

The TGA instrument measures weight change of a sample as a function of temperature.


This service is also relevant in: Metrology, Plastics, Textiles

Service details

Service
Thermogravimetric Analysis (TGA)
Metrology Area
Mass / Weight, Temperature
Delivery level
Accredited, Non-accredited
Standards

ISO 11358-1, SP method 1390

Price
Price on tender
Delivery time

Delivery time is within two weeks from sample arrival at RISE laboratory. 


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Emelie Andersson

Forsknings- och utvecklingsingenjör
+46 10 228 49 57 Read more about Emelie

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Anna Bondeson

Forsknings- och utvecklingsingenjör
+46 10 516 55 30 Read more about Anna

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Purpose

Composition of basically any material may be determined between 50°C and around 1000°C. Typically we analyse plastic- and rubber materials, but we are also pleased to analyse fibers, textiles, varnish, adhesives, biofuels or other materials. The most common analyses are composition of a material or a product. 

 TGA is used for: 

  • Analysis of composition
  • Determination of residue, ash content or inorganic filler
  • Thermal stability or oxidation stability 

Information from TGA analyses are for example moist content in a material (water evaporate at 100°C), presence of low molecular oils and plasticizers in polymers or inorganic fillers, i.e. residual ash. 

Method

A small sample is placed in the instrument chamber, an oven equipped with a scale and controlled temperature and atmosphere. Oxygen, air or nitrogen is chosen as purge gas and the temperature program may be either dynamic or isothermal, depending on the analysis. 

The test samples are small, only 5-15 mg is needed and the analysis takes a couple of hours depending on the chosen temperature program. In nitrogen atmosphere a plastic sample is pyrolyzed, i.e. thermally decomposed. If the purge gas is shifted to air or oxygen organic (carbon containing) substances are incinerated. 

We use standard test methods as well as tailor-made analyses. We have long experience in designing test methods. 

TGA instruments are found at different locations within RISE and we collaborate to give you as a client the best service and delivery time. In Mölndal we have long experience and expertise on recycled plastics and material development, in Borås we have expertise in anlayses of plastic construction materials, rubber  and durability, in Göteborg plastic pipe materials are analysed, and in Stockholm/Kista the expertise on plastic materials in chemical corrosive applications are found.

Deliveries

A report containg information about test method, used equipment, with enclosed thermograms and explanation of the results.