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In-situ Scanning electron microscope

In‑situ SEM enables real-time studies of microstructural changes under controlled reactive enviroments. The technique is unique and makes it possible to follow, for exaple, the combustion and ash formation och a carbon-based materal, or the sintering of a lime-based material.

At RISE in Piteå, there is a Apreo 2S Hi-Vac SEM (Scanning Electron Microscope) from Thermo Fisher. To optimize the analysis of different types of samples, the instrument is equipped with several detectors:

  • ETD – Everhart-Thornley Detector.
  • T1, T2 och T3 - In-lens trinity detectors.
  • CBS/ABS – BSE-detector
  • STEM – Scanning Transmission Electron Microscopy
  • EDS – Energy Dispersive X-ray Spectroscopy for elemental analysis

In addition to these detectors, the instrument is equipped with:

  • µHeater - Enables studies of a sample during heating up to 1200 °C, with extremely fast heating rates up to 10 000 °C/s
  • µReactor – In addition to the heat function, a sample can simultaneously be studied in a specific gas atmosphere, such as nitrogen, oxegen, hydrogen, carbon dioxide etc.

References from previous work:

Calcination of CaCO3 and the subsequent sintering/densification of CaO directly visualized with in-situ SEM

Facts

Test & Demo name

In-situ SEM

Industry

Materials

Area

Biorefinery

Region

Region Norrbotten

Therese Vikström

Contact person

Therese Vikström

Forsknings-och utvecklingsingenjör

+46 10 516 62 01

Read more about Therese

Contact Therese
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