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The National Laboratory for Chemical Metrology

National Laboratory Chemical Metrology
The National Laboratory for Chemical Metrology

RISE is the National Metrology Institute of Sweden and is responsible, through its National Laboratories, for the fundamental measurement quantities in the International System of Units SI.

At the national laboratory for chemical metrology, we work with measurement quality and quality assurance in the chemical area. We develop sampling and measurement methods and guidelines for measurements from Eurachem, among others. Collaboration with other laboratories, interest organisations and authorities around the world is important to promote the development of a structured metrology system in the field of chemistry, both nationally and internationally.

International comparison measurements

We are constantly developing measurement methods that respond to industry and society's needs for quality-assured measurements. We conduct experimental activities around reference measurements, for example determination of elements, characterisation of ultrapure water and in energy gases. We collaborate with other leading institutes worldwide in various research projects and regularly participate in international comparison measurements to ensure the quality of our measurements.

We offer:

  • Quality assured measurements in energy gases.
  • Training of laboratory personnel through courses in measurement uncertainty, method validation and quality control.
  • Development of methods for elemental analysis, including specification of constituent elements.
  • Calibration of conductivity instruments for ultrapure water and liquids with high salinity.

Karine Arrhenius

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+46 70 567 57 28 Read more about Karine

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Division (OLD): Division Safety and Transport Division: Division Safety and Transport National Metrology Institute Sekundär områdes navigation: Metrology

Benefits of new lead-free bullet demonstrated

Staffan Leths led free bullets

He has developed copper-based hunting bullets that work just as well or better than those containing lead. Staffan Leth, hunter and passionate sport shooter, has the best possible proof of this. RISE’s test facility has delivered impartial evidence of the bullet’s behaviour.

Lead is a major problem when it ends up in our food and in nature. Even in very small amounts, the metal can cause damage to the nervous system, especially in foetuses and young children. 

It is no wonder that society limits its use in various ways. Lead bullets and lead shot, which are used in hunting, result in 10-16 tonnes of lead ending up in nature every year. A total ban is already being debated. 

Other lead-free bullets do not work optimally 

“For me, the lead issue arose already around 1990, when people started talking about how lead in gaseous form can be harmful, and that those of us who shoot firearms a lot would need to get tested,” says Staffan Leth, whose life has revolved around weapons in various ways. Raised in Djurås between Leksand and Borlänge, hunting and sport shooting have always been central. 

Staffan’s shop, which was started as a hobby in the ’90s, currently has three employees and stocks a wide range of goods. And lead has been an ever-present issue. 

“There have been alternatives, but they have not worked satisfactorily,” says Staffan. “In 2018, I therefore started to develop a lead-free hunting bullet – and it works better than traditional lead-nose bullets.” 

Staffan is used to so-called handloading products, which is when hunters or shooters adapt their ammunition to their firearm. Handloading (or, more accurately, reloading) involves reusing previously fired casings or shells by inserting a new percussion cap, gunpowder, and slug, which is done using a special tool available for each calibre. Developing a completely new bullet required a lot of careful planning and numerous attempts. 

“When I started the development, I had a high ambition: to make the world’s best hunting bullet. In Sweden. Lead-free. And with the same precision as a professional bullet! All with a price that appeals to every Swedish hunter.” 

An ambitious goal, especially since the lead-free alternatives available on the market are often perceived as inferior. 

“The quality has varied. Many hunters have been sceptical and found that they do not expand enough on impact. They also claim that they travel sluggishly through the barrel, which builds gas pressure that results in more powerful recoil.” 

When I started the development, I had a high ambition: to make the world’s best hunting bullet. In Sweden. Lead-free.

Copper alloy with optimal design 

The bullet Staffan has now developed has a copper alloy and a design that he believes works optimally. 

“It has good expansion and expands up to double the diameter. Another advantage is that the residual weight is 99-100 percent.” 

The latter is an advantage even compared to traditional lead bullets, as it means that the bullet holds together inside the wound and does not spread small fragments that contaminate the meat. A lead-nose bullet fragments considerably, which means that you have to cut away a lot of meat around the entry point to ensure that lead residues do not end up on your plate. 

“Those who use our bullet claim to have 10 percent less waste compared to when they use lead bullets,” says Staffan. “For those who sell game meat and shoot many animals every year, that translates to many additional kilograms of meat that can be eaten, as well as more money.” 

To test his bullet, Staffan used ballistic gelatin, designed to simulate the effects of bullet wounds in animal muscle tissue. He feels confident in his conclusions. 

“But I need to verify my claims, both by having an independent party perform the same shooting tests and by demonstrating how the bullet behaves on impact.” 

He therefore approached RISE, which has a flexible test facility that allows for customisation according to the relevant ballistic requirements. During testing, a high-speed camera recording at 15,000 frames per second was used to evaluate the bullet’s behaviour. You can see an example in the video below. 

Received impartial evidence of the functionality 

“I got impartial evidence that the bullet actually works. They conducted rigorous tests and gave me videos showing the bullet’s behaviour.” 

Staffan has already started selling his lead-free bullet in several countries, and in the autumn of 2022 he also developed his own ammunition. The next step will be for other manufacturers to start using the bullet as a lead-free alternative in their ammunition. 

“Given that the ban is already enforced in some regions, it feels great to have a bullet that I believe is better than traditional lead bullets – and that we have been able to demonstrate this with the help of an impartial operator,” says Staffan. 

Here is an example of the videos recorded with RISE’s high-speed camera of Staffan Leth’s lead-free hunting bullets. The video shows how the bullet, a 308 calibre Winchester, behaves and how the top ‘mushrooms’ out into the ballistic gel that corresponds to muscle tissue. It allows RISE to measure several different parameters, such as the velocity of the bullet on impact and the trajectory of the bullet before it stops.

LEAD IS A PROBLEMATIC METAL 

It is estimated that up to a million birds, which peck at lead shot, die of lead poisoning every year. In early 2023, the use of ammunition in the form of lead gunshot when shooting on wetlands was therefore prohibited in the EU. Sweden has had a similar ban since 2006, but the new rules are more extensive.  

Work is underway in the EU to expand the restriction on lead. According to the proposal, the ban would also cover lead in ammunition (both shot and bullets) used in hunting outside wetlands and in shooting sports. In addition, a ban has also been proposed on the use of lead in fishing gear, such as sinkers and fishing lures. 

(Source: Swedish Chemicals Agency) 

ABOUT RISE’S TEST FACILITY 

RISE’s state-of-the-art test facility north of Varberg performs tests on bullet-proofing and impact-resistance for all types of operations. Small and medium-sized enterprises often utilise the facility during the development or testing phase of their products and services. The shooting range is flexible and can be customised to the relevant ballistic requirements and standards with high safety and confidentiality. The operations are SUA-classified (which relates to protective-security procurement) and accredited by Swedac. 

The facility can be used for a variety of tests and can even accommodate entire vehicles. 

Glenn Langvik

Marknadschef
+46 10 516 58 60 Read more about Glenn
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Sustainability: 9. Industry, innovation and infrastructure Physical protection and safety Sekundär områdes navigation:
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Chemical analyses crucial for increased gas use

Gas analysis

Energy gases such as hydrogen, biogas and biomethane, and methods for storing and using carbon dioxide play an important role in the climate and energy transition. Different areas of use have different requirements on the quality and composition of the gases, which requires chemical analyses and quality-assured measurements.

Energy gases are important not least in the transport sector, which aims to be fossil-free by 2030. Hydrogen can, for example, be used in fuel cells, which is a clean technology with water vapor as the only residual product. Biogas and biomethane also have many advantages in the transition. However, if the gas used is not of the correct composition or purity, it can cause operational problems and serious damages.

“Gas accounts for 20 percent of energy in Europe today but have an even greater potential. In addition to the environmental aspects, Europe can also become more independent by producing more biogas and biomethane instead of importing natural gas. At the same time, chemical analyses of energy gases is a relatively new field that has only developed properly in the last ten years”, says Karine Arrhenius, researcher at RISE who works with chemical analyses and development of quality-assured measurement for energy gases.

Composition and purity requirements

For each area of use, there are specifications with requirements on the quality, composition, and purity of the gas. These requirements exist to protect health or equipment, but also to allow the systems to function optimally. To ensure that the gas meets the requirements, chemical analyses, and quality-assured measurements are required.

“This in turn requires reference material, quality-assured sampling, standards and of course, analysis methods”, says Karine Arrhenius.

Laboratory comparisons important for quality

A large part of the development of these methods and standards takes place in collaboration with European colleagues in projects that RISE both participates in and coordinates. RISE has been involved in developing new ISO standards that are expected to be published next year and has been involved in developing a platform with an overview of various European laboratories that offer services linked to energy gases. RISE both participates in and arranges European laboratory comparisons, which are important for maintaining quality in the laboratory. The participating laboratories analyse a reference gas with a known composition and purity. The results are then compared.

“These comparisons are the best way to show the laboratory’s ability and reliability. It is also a requirement for accreditation to participate in such comparisons. Right now, we are organising two comparisons, one with hydrogen with 13 participating laboratories, and one with biomethane.

We could, for example, use the carbon dioxide produced in greenhouses or to produce carbonated drinks

Karine Arrhenius.

In addition to chemical measurements, RISE also works with measurements of gas flow, which is needed in areas such as calibrating flow meters at gas stations, and with testing sensors to be able to handle the gases in a safe way. The sensors can be used to trigger alarms, activate ventilation, or shut down systems to prevent flammable levels of gases. During the production of energy gases, carbon dioxide is also formed which needs to be taken care of, either by storing it (CCS, Carbon Capture and Storage) or by using it (CCUS, Carbon Capture Utilisation and Storage).

“We could, for example, use the carbon dioxide produced in greenhouses or to produce carbonated drinks. Here, too, there are specifications that require chemical analyses”, says Karine Arrhenius.

New questions and problems

Most measurements and analyses take place in a laboratory environment, but field measurements also occur. Some measurements take place online, i.e., while a production process is in progress. For Karine Arrhenius, this means a never-ending stream of questions and problems that need to be solved.

“We develop new analysis methods through new research, which creates new services for customers, new services bring new customers who have new questions. I have sometimes wondered when there will be a point where no new questions can be found, but it doesn't seem to be coming. There are new gases to be analysed, new mixtures, new standardisation needs, new methods to be developed”, says Karine Arrhenius.

Karine Arrhenius

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+46 70 567 57 28 Read more about Karine

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Last published: Chemical and biological analysis Sekundär områdes navigation:
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Energy and electrification

Fire testing of batteries - battery testing

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Fire testing of batteries - battery testing Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

The purpose of fire testing of batteries is to investigate the safety and performance of a battery under various conditions. This is a kind of safety-critical testing that often leads to severe fire and, in some cases, explosion.

Purpose/Benefit:

Before a battery is approved for use and put into service, it needs to be tested for fire testing and thermal propagation. This type of battery testing is an important part of battery development and is included in several battery standards.

What is fire testing of batteries?

Fire testing of a battery involves exposing the battery to open flames from an external fire for a period of time. This simulates a situation where the battery catches fire, which can occur during use. Such a situation could be, for example, in a vehicle crash or when there is a fire in a stationary energy store. An important part of fire tests is to see how the cells in a battery are protected by the enclosing casing.

Method (what/which methods are used to perform the service):

We perform fire tests on batteries in our safety critical testing lab. The lab has a large capacity and can house testing objects up to the size of a full-scale vehicle. The lab has extra thick walls, thick reinforcement and steel doors, allowing us to safely handle testing up to 8 MW. As the test environment is indoors, the environment is controlled and constant, which allows for repeatable tests and reliable results.

We offer sustainable fire testing

Fire testing causes toxic gases such as carbon monoxide, nitrogen dioxide, hydrochloric acid, hydrofluoric acid, hydrogen cyanide, benzene and toluene. In addition to safely handling these toxic and flammable gases, we make sure to minimize the environmental impact of our testing. Flue and gas are taken care of in our unique flue gas cleaning facility. We collect the extinguishing water from the test, and separate hazardous particles and send them to a landfill. All to test in the most possible sustainable way. 

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

You will receive a digitally signed technical report with test results. The report can be delivered in either Swedish or English.

On our area page for batteries you can read more about our work within batteries.

Here you can read more about safety-critical battery testing at RISE.

Area: Batteries Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Magnus Ling
Patrik Johansson, Affärsutvecklare
Batteries at RISE - fire and thermal propagation testing
Field measurements: No Price type: 1 Division: Division Safety and Transport Preparation: No preparation required Link to order form: Contact us Standards:

UN ECE R100
GTR 20
GB38031-2020
KMVSS-Art 18-3
SAE J2464
UL2580

Certification and marking: Other Certifications Type of service: Testing / Analysis / Evaluation Instrument: Voltage references General area:
Electricity
Combustion
Temperature
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CE-marking, lifting accessories and lifting machinery

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): CE-marking, lifting accessories and lifting machinery Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

Lifting accessories and lifting machinery are covered by the Machinery Directive, 2006/42/EC and shall be CE marked. For certain types of lifting accessories, there are harmonised standards that can be followed to meet the requirements of the Machinery Directive.

Purpose/Benefit:

RISE has extensive experience of CE marking of lifting accessories and lifting machinery. Our broad expertise enables us to offer our customers support relating to CE marking, either throughout the complete process including testing, or e.g., to determine applicable requirements or standards.

Examples of standards

EN 13155 Cranes - Safety - Non-fixed load lifting attachments

Method (what/which methods are used to perform the service):

EN 13157 Cranes - Safety - Hand powered cranes

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

ISO 12100 Safety of machinery — General principles for design — Risk assessment and risk reduction

Area: Testing Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Per Landström, Projektledare
Jukka Holappa, Enhetschef
Lift
Field measurements: No Price type: 1 Division: Division Materials and Industry Preparation: No preparation required Link to order form: Contact us Standards:

EN 13155 Cranes - Safety - Non-fixed load lifting attachments

EN 13157 Cranes - Safety - Hand powered cranes

ISO 12100 Safety of machinery — General principles for design — Risk assessment and risk reduction

Certification and marking: Other Certifications Type of service:
Certification
Testing / Analysis / Evaluation
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Model manufacturing

Model manufacturing
SSPA model manufacturing

Our facilities for designing, building and outfitting of models for all kinds of model tests include milling machines for hulls and propellers, paint box, a team of measurement engineers and a workshop for the assembly of hulls, propellers, rudders and other appendages.

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The superb flexibility of RISE milling system for large objects makes it one of the best systems for manufacturing ship models, and patterns. Unique programming with effective handling of various process tools enables the production of the most demanding shapes. The robot milling system can be used for model and prototyping for any object up to a length of 12 meters, height of 2.5 meters and beam of 2.5 meters.

For propeller manufacturing a 5-axis CNC milling machine is used. With the 5 axis technique propeller can be milled with high accuracy. Propellers are made of bronze. 

Hull models are manufactured in a foam plastic material to ensure a stable hull form over time and with varying temperatures and humidity.

Propellers and models are laser measured on a regularly basis to ensure high accuracy, in accordance with ITTC tolerances.

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Maritime
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Division (OLD): Division Safety and Transport Maritime Sekundär områdes navigation: Metrology

Maritime Dynamics Laboratory

Maritime Dynamics Laboratory
SSPA Maritime Dynamics Laboratory

The Maritime Dynamics Laboratory (MDL) at RISE test facility SSPA Maritime Center is one of the world's largest wave laboratories, 88 x 39 meters with a depth of 3.5 meters. It is used for tests of how different types of vessels behave in varying wind and wave conditions. The model tests are of great importance for the development of new vessels.

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The MDL can also be used for assessing maneuvering properties in waves. Model tests in oblique wave conditions play an important part when developing new hull forms for surface vessels. The angle of roll, degree of deck wetness, and course-keeping qualities of a vessel in bow, beam, and stern quartering seas are parameters that are difficult to predict accurately from theoretical calculations alone. Model tests in oblique seas, combined with simulations, have proved to be valuable tools in the study of ship projects.

The computer controlled, multi-motion carriage, spanning the whole basin, offers unique possibilities for conducting captive or free sailing maneuvering tests. In captive maneuvering tests, the facility can be used to perform both large-amplitude PMM tests and rotating arm tests, without having to change the set-up between the tests.

For free sailing tests, the width of the basin allows most maneuvers to be performed with fairly large models, thus reducing the influence of scale effects. The MDL is also a very useful tool when determining whether a new or existing project fulfils the IMO regulations concerning turning ability and yaw checking. Course keeping abilities can also be studied.

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Division (OLD): Division Safety and Transport Maritime Sekundär områdes navigation:
Metrology
Sensors and sensor systems
Production and manufacturing

Cavitation tunnel

Cavitation tunnel
SSPA cavitation tunnel

RISE cavitation tunnel at the test facility SSPA Maritime Center consists of three interchangeable measuring sections allowing high speed testing of propellers up to 23 m/s as well as large ship models of up to 10 meters. When performing cavitation studies for ships, the complete ship model can be installed.

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The cavitation tunnel is a very cost-effective facility, and so there are many possibilities for solving any problems that might occur. In addition to cavitation studies and erosion prediction, the tunnel is used to measure pressure pulses and radiated noise. Tests can be performed for all kinds of vessels, including merchant ships and fast naval ships, as well as submarines and other underwater vehicles. In addition to study the ship propeller also energy saving devices, rudders, fins and PODs can be included in the scope.

The cavitation tunnel, with its three interchangeable sections, is also very valuable in various types of flow studies. Well correlated traditional methods are combined with high-speed video, PIV etc. Both in-house and external tools and programs are available to analyze the results.

The cavitation tunnel can also be used for studying and developing the latest green technologies such as ships equipped with an air cavity, air lubrication of ship hulls and tidal water turbines.

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Maritime
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Division (OLD): Division Safety and Transport Maritime Sekundär områdes navigation:
Power production
Metrology

Towing tank

Towing tank
SSPA towing tank

The towing tank at RISE test facility SSPA Maritime Center has many applications, primarily concerning hull and propeller form optimization for all kinds of ships or energy saving devices with respect to resistance/ propulsion. A database containing over 8,000 ship hull forms provides the basis for the result analysis.

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The tank dimensions and the high carriage speed facilitate the use of large, self-propelled displacement models and testing of high-speed vessels (mono- and multihulls, semi-planing and planing craft, surface effect ships, etc.).

The flap type wave generators provide regular as well as irregular waves for the determination of seakeeping characteristics and ride comfort. By combining the results with a SSPA Seaman Simulation behavior in oblique seas can be estimated. Arrangements and techniques for testing submersibles (submarines and other underwater vehicles), sailing boats, and fishing gear are available, and various unconventional objects can also be investigated.

A database containing over 8,000 ship hull forms provides the basis for result analysis and guidance for hull form optimization of merchant ships, as well as high-speed and planing crafts. In-house research activities ensure enhanced knowledge and the continuous development of methods within the field of ship hydrodynamics.

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Division (OLD): Division Safety and Transport Maritime Sekundär områdes navigation:
Metrology
Total defence and crisis preparedness

Immersion test of batteries – battery testing

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Immersion test of batteries – battery testing Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

To immersion test batteries means immersing a battery in a liquid, and then evaluating how it is affected. After test, any damage to the battery is examined. This is important to ensure that batteries have sufficient protection against external impact.

Purpose/Benefit:

Battery immersion is when a battery is immersed in a liquid for a time period from a few minutes to several days. During the test, the battery must not break, burn or explode. After the immersion, the battery is removed and accuartely examined for internal and external damage. The test results show the battery´s performance, stability and life span.

Why immersion test a battery?

The immersion test of batteries is done to check the battery's resistance to liquid short circuits, corrosion, and oxidization. Immersion tests ensure that the battery fulfills the usage requirements. Immersion is included in several different standards for batteries, for instance, in SAEJ2464, UL2580, and J2929.

Method (what/which methods are used to perform the service):

Static immersion test

In static immersion tests, the battery is immersed in a liquid for a set period, often 24-48 hours. When the time has elapsed, the battery is removed and inspected for internal and external damage, such as corrosion, leakage, and oxidization. 

Cyclic immersion test

In the cyclic immersion test, the battery is immersed in a liquid for a set period. The battery is then removed and allowed to dry at room temperature. The immersion, retrieval, and drying sequence is repeated several times. 

Immersion test - High temperature

In the high-temperature immersion test, the battery is immersed in a high-temperature liquid. This will show if the battery can be used in a high-temperature environment.

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Reliable immersion test results

By hiring RISE for immersion tests of batteries, you get access to tests in a controlled, indoor environment. This means that temperature, humidity and other environmental conditions are constant. The controlled climate ensures reliable results.

You get impartial immersion testing

Our testing is objective and unbiased, as RISE is an independent, government-owned research institute. As an external test provider, we have no connection to the product manufacturer - thus, there is no risk of conflict of interest. When you test with us, you get the test results presented clearly and objectively, making it easier for you to take the results further for product development or market introduction.

Area: Batteries Contact person (Enter one name per field. Activated personal contact pages will appear automatically): Magnus Ling
RISE-batteries-coworker-working-at-laptop
Field measurements: No Price type: 1 Division: Division Safety and Transport Preparation: No preparation required Link to order form: Contact Magnus Standards:

SAEJ2464
UL2580
J2929
GBT38031
ISO6469
KMVSS

Certification and marking: Other Certifications Type of service: Testing / Analysis / Evaluation Instrument:
Electricity meters
Vibration measurement equipment
General area:
Electricity
Sound and vibrations
Temperature
Time and frequency
Order information: Would you like to learn more? Divison (OLD): Division Safety and Transport Delivery level: Accredited
magnus.ling@ri.se,
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9. Industry, innovation and infrastructure
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Purpose - Header: What is immersion test batteries? Metod - Header: The most common immersion tests Delivery - Header: Immersion testing at RISE
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