Jump directly to content

Analysis of materials and surfaces with imaging mass spectrometry

Chemical surface analysis with ToF-SIMS
Photo of ToF-SIMS instrument

Do you want to know what is on your surface or more about your new material? With our unique expertise in imaging mass spectrometry (ToF-SIMS), we can provide molecular information about material surfaces and image the spatial distribution of different components on a surface. 

Do you want to know what is causing discolorations on your surface? Or know more about your newly developed material? RISE offers unique expertise and equipment for molecular analysis of surfaces and materials with Time-of-Flight Secondary Ion Mass Spectrometry (ToF-SIMS), from smaller analysis assignments to longer research and development collaborations. With ToF-SIMS we can measure very low amounts of sample and imaging specific molecules, including organic ones, at very high spatial resolutions, something that is not possible with other analytical methods. With our long experience in answer questions about surfaces and materials in a variety of industrial areas, we have unique expertise to answer your specific question.

Examples of questions and analysis tasks we can help with are: 

  • Problem solving for manufacturing industry in various areas, e.g.
    • adhesion problems
    • discoloration
    • coatings
    • cleaning / contamination problems
  • Characterization of advanced / composite materials for examining the spatial distribution of components, e.g.
    • additives in polymers
    • surface coatings or layered materials
    • functionalized surfaces
    • pharmaceutical formulations (for example, tablets)
    • batteries
  • Analysis of complex natural materials, e.g.
    • biological tissues
    • geological samples
    • paper and wood
  • Chemical analysis of particles
    • single particles down to 10-100 µm diameter can be analyzed

Peter Sjövall

Forskare
Read more about Peter

Contact Peter

CAPTCHA

* Mandatory 

By submitting the form, RISE will process your personal data.

Sandra Siljeström

Forskare
+46 10 516 52 69 Read more about Sandra
Profile image

Contact Sandra

CAPTCHA

* Mandatory 

By submitting the form, RISE will process your personal data.
Division: Division Materials and Industry Chemical and biological analysis

Waste Sorting Analyses

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Waste Sorting Analyses Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

A tool for supporting the development of strategies for reducing the climate impact and increasing material recovery.  

Purpose/Benefit:

Sorting analysis is a strategic approach used to assess the quality of waste streams by examining the composition of various waste fractions such as combustible waste, plastic, wood, and paper. The data gathered through this process enables to:

  • evaluate the efficiency of source sorting and its potential for material recycling
  • determine the quality of source sorted waste fractions
  • explore the potential in post-sorting plants
  • identify opportunities for improvement in post-sorting facilities
  • explore the potential for Carbon Capture and Storage (CCS) and Carbon Capture and Utilisation (CCU)
  • assess the feasibility of implementing differentiated gate fees for incineration
Method (what/which methods are used to perform the service):

We can help you with:

  • Tailor-made sorting protocols based on your needs.
  • Planning and coordination of sorting analyses of different waste streams.
  • Extended sorting analyses in specific fractions i.e. plastic waste. 
  • Residual household waste, source sorted fractions for material recycling i.e. plastic packaging, commercial and industrial waste, construction and demolition waste or bulky waste from households or recycling centres are among the waste streams we can help you with. 

We also offer a range of services connected to the outputs from the waste sorting analyses:

  • Analyses of parameters such as fossil/biogenic carbon content, fuel quality; hazardous substances (i.e. PFAs) and trace element analyses
  • Estimation of CO2 emissions from incineration of waste streams. 
  • Identification and quantification of polymer types

Technical economical assessment 

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

.

Delivery time:

Depends on the scope of the project. 

Area:
Circular transition
Energy
Packaging
Plastics
Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Mar Edo
Carl Jensen, Projektledare
commercial and industrial waste
Field measurements: Yes Price type: 1 Division: Do not use - Division Built Environment Preparation: Description of preparation Preparation information:

The client is responsible for taken representative samples. RISE can guide in this process. 

Certification and marking: Not applicable Type of service: Testing / Analysis / Evaluation Instrument: Not applicable General area: Not applicable Delivery level: Not applicable
mar.edo@ri.se,carl.jensen@ri.se
/en/node/10120
7. Affordable and clean energy
Purpose - Header: How can sorting analyses help you? Metod - Header: Our offer Delivery - Header: Do you want to know more? Contact us More information - Header: Mer information
Order
form
Circular transition Sekundär områdes navigation:
Energy and electrification
Plastics
Chemical and biological analysis
Tjänstetyp tagg: Provning

Fibre analysis, selection of SS-EN ISO 1833, ISO 21915-2, SS-EN ISO 20705, ISO/ TR 11827

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Fibre analysis Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

The need to be able to identify fibres is increasing as textile recycling advances. RISE can offer a selection of different fibre analysis methods for both new and recycled synthetic and natural fibre types. 

Purpose/Benefit:

Being able to identify fibres can be crucial for subsequent processes. RISE provides both quantitative and qualitative methods for textile fibre identification.

Method (what/which methods are used to perform the service):

RISE offers: 

  • Chemical Analysis: We use specific solvents to dissolve certain fibres, allowing for precise determination of the remaining fibre types.
  • Microscopic Analysis: Through microscopy, we identify and quantify the fibre content in textile samples. Dyeing before microscopy can be used to distinguish certain types of cellulose.
     
Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Normal delivery time is 10-15 working days.

Area: Textile Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Carina Berglund, Forskare
Desiré Rex, Forskare
blue colored fibres
Field measurements: No Price type: 1 Division: Division Materials and Industry Preparation: No preparation required Standards:

SS-EN ISO 1833 Textiles - Binary fibre mixtures - Quantitative chemical analysis

ISO 21915-2 Textiles - Qualitative and quantitative analysis of some cellulose fibres (lyocell, cupro) and their blends - Part 2: Blend quantification using light microscopy method

SS-EN ISO 20705 Textiles - Quantitative microscopical analysis - General principles of testing

ISO/TR 11827 Textiles - Composition testing - Identification of fibres 

ISO 137 Wool - Determination of fibre diameter - Projection microscope method

SS-EN ISO 1973 Textile fibres - Determination of linear density - Gravimetric method and vibroscope method

SS-EN ISO 5079 Textile fibres - Determination of breaking force and elongation at break of individual fibres 

SS-ISO 6989 Textile fibres - Determination of length and length distribution of staple fibres (by measurement of single fibres)

Certification and marking: Not applicable Type of service: Testing / Analysis / Evaluation Instrument: Not applicable General area: Not applicable Delivery level: Not applicable
carina.berglund@ri.se,desire.rex@ri.se
/en/node/9710
Purpose - Header: Purpose Metod - Header: Fibre analysis Delivery - Header: Delivery More information - Header: Mer information
Order
form
Textiles Sekundär områdes navigation:
Circular transition
Metrology
Chemical and biological analysis
Tjänstetyp tagg: Provning

Support for cleaning PFAS-contaminated firefighting equipment

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Support for cleaning PFAS-contaminated firefighting equipment Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

When transitioning to PFAS-free extinguishing agents, there is a risk that the new, fluorine-free extinguishing agent becomes contaminated due to PFAS remaining in the system. It is therefore important to clean the system before refilling and to ensure adequate cleaning.

Purpose/Benefit:

The transition to fluorine-free (PFAS-free) extinguishing agents is underway in society. In many cases, simply replacing the firefighting foam concentrate is not sufficient; there is a risk that PFAS remaining in the system will contaminate the new extinguishing agent, perpetuating the spread of PFAS. Before refilling with new extinguishing agent, it is important to conduct thorough cleaning and ensure that it successfully removes PFAS from surfaces. Research conducted shows that despite repeated flushing, PFAS continues to persist in the system.

Method (what/which methods are used to perform the service):

RISE has the expertise to provide support for cleaning PFAS-contaminated equipment. In a recently completed research project, we have gained knowledge about cleaning methods. RISE also possesses knowledge about current and upcoming regulatory requirements. We have the capability to provide recommendations for analyses to ensure adequate cleaning and to conduct these PFAS analyses.

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Delivery according to request and agreement.

Area: Risk and safety Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Sixten Dahlbom, Projektledare
Tove Mallin, Enhetschef
Laboratory test
Field measurements: Yes Price type: 1 Division: Division Safety and Transport Preparation: No preparation required Certification and marking: Not applicable Type of service: Testing / Analysis / Evaluation Instrument: Not applicable General area: Not applicable Delivery level: Not applicable
sixten.dahlbom@ri.se
/en/node/9710
9. Industry, innovation and infrastructure
Purpose - Header: Cleaning of PFAS-contaminated firefighting equipment. Metod - Header: Analytical services and expertise Delivery - Header: Delivery More information - Header: Mer information
Request for quote
form
Fire safety Sekundär områdes navigation:
Risk and security
Chemical and biological analysis
Tjänstetyp tagg: Konsultuppdrag

Measurement quality among atoms, ions and molecules

Measurement quality among atoms, ions and molecules

Do you want to learn more about chemical analyses, what uncertainties exist and how chemists try to deal with it in their quality work?

All measurements have challenges that affect the quality of the results. Typical for chemical analyses is that you handle a large number of measurement quantities, have many different sample types with different compositions and that the result is often affected by the sample preparation.

Eskil Sahlin, researcher at RISE, will hold this seminar and talk about the challenges of chemical analyses, about the measurement uncertainty in the measurements and about how chemists can handle the challenges through methodical quality work. 

The cost of your own booked digital lecture, about an hour long incl. question time/discussion, is 8 715 SEK regardless of how many you are. The lectures are offered in Swedish or English.

Viktoria Jonasson

Projektledare
+46 10 516 56 39 Read more about Viktoria
Profile image

Contact Viktoria

CAPTCHA

* Mandatory 

By submitting the form, RISE will process your personal data.

Lena Gamalielsson

Administratör
+46 10 516 60 02 Read more about Lena
Profile image

Contact Lena

CAPTCHA

* Mandatory 

By submitting the form, RISE will process your personal data.
Interest inquiry
mtkurs@ri.se
/en/about-rise/operations/mission-governance/policy-documents/privacy-policy
Division: Division Safety and Transport

'Black mass' analysis for battery recycling

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): 'Black mass' analysis for battery recycling Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

To pave the way for optimizing battery recycling processes, a proper analysis of ‘black mass’ and spent battery components before and after recycling is very important. 

Purpose/Benefit:

‘Black mass’ is the industry term used to describe the product obtained from crushing and shredding spent Li-ion batteries. It comprises a mixture of elements, including graphite, lithium, manganese, nickel, cobalt, electrolyte, separator, impurities, etc. 

A comprehensive analysis protocol is essential for evaluating the black mass derived from various battery chemistries. This protocol should encompass all necessary property assessments before and after the recycling process. By identifying potential hazards and mitigating associated risks, the protocol ensures safe and efficient recycling operations.

Method (what/which methods are used to perform the service):

Explore our Characterization 

  • Metals and impurities: The determination of compositions in ‘black mass’ and related materials  can be effectively carried out using techniques such Inductively Coupled Plasma - Optical Emission Spectrometry ICP-OES, Inductively Coupled Plasma - Mass Spectrometry ICP-MS, X-ray fluorescence XRF.
  • Level of moisture: The level of  moisture in the ‘black mass’ is determined using titration.
  • HF-content: The content of HF can be determined using titration.
  • PF6-content: The content of PF6 can be determined using Ion Chromatography, IC.
  • Morphological analysis and particle size determination:  The morphological characteristics, grain size, and composition can be determined using Scanning Electron microscopy SEM+EDS
  • Electrolyte analysis using Gas chromatography–mass spectrometry GC-MS:

Gas chromatography-mass spectrometry is an analytical technique that is highly effective for analyzing ‘black mass’ such as determining the composition of carbonates. For example ethylene carbonate, propylene  carbonate, diethyl carbonate, ethyl methyl carbonate etc. 

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Report and results

Area: Batteries Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Moufida Mansouri, Senior researcher
Fredrik Solhage, Enhetschef
Black mass samples
Field measurements: No Price type: 1 Division: Division Materials and Industry Preparation: No preparation required Certification and marking: Not applicable Type of service: Testing / Analysis / Evaluation Instrument: Not applicable General area: Not applicable Delivery level: Non-accredited
moufida.mansouri@ri.se,fredrik.solhage@ri.se
/en/node/9710
Purpose - Header: Purpose Metod - Header: Methods Delivery - Header: Delivery More information - Header: More information
Request for quote
form
Batteries Sekundär områdes navigation:
Circular transition
Metrology
Chemical and biological analysis
Tjänstetyp tagg: Provning

High-resolution wood characterisation ensures a sustainable future

High resolution wood characterisation

The unique laboratory in Stockholm generates a lot of data every year to investigate the effect of environment and genetics on wood properties together with other institutes and universities. At the same time, the laboratory is constantly developing its ability to analyse new sample types and generate new data types.

In the early 2000s, investment was made in SilviScan, a system capable of anatomical characterisation (Figure 1) and high resolution density and microfibril measurements from pith to bark on samples from pulleys and 10 mm diameter cores. This installation is one of only three such measurement systems in the world. Complementing the measurement system, there were also sample preparation tools that can prepare samples of appropriate size and surface quality with high precision. The system in Stockholm has since been an important tool in tree breeding and research projects investigating the effect of genetics and environment on wood properties.

Figure 1: SilviScan performs, among other things, anatomical
analyses. While research on forest resources has traditionally focused on wood properties important for pulp and timber products, in recent years there has been increased interest in other bioproducts where the chemical composition is more important than the physical.

Consequently, it also invested in a near-infrared (NIR) camera for chemical characterisation of both pulleys and drill cores. This particular combination of the NIR camera with SilviScan makes the laboratory unique in its ability to characterise wood samples in their chemical and physical properties.

At the same time, the number of greenhouse experiments on hybrid aspen, which is often used as a model tree in scientific studies, increased in order to quickly investigate genetic and environmental effects on wood and tree characteristics. In these greenhouse studies, new wood samples are generated in just three months, but the laboratory was more equipped for the analysis of pulleys and 10 mm drill cores from adult trees. Consequently, the development of a sample preparation routine for greenhouse samples was initiated that includes NIR scanning of trunk cross-sections followed by sawing and scanning with SilviScan. Thus, the laboratory is now able to generate high-resolution chemical and physical information on greenhouse samples that are also generated at a high rate.

In a further step towards wood characterisation of younger trees - this time ca. 8-12 year old spruce field trials - sample preparation and scanning procedures were recently developed for the analysis of 5 mm diameter cores taken just above the ground, instead of at breast height. In contrast to analyses on older trees, this means that only juvenile wood is analysed, which is often regarded as the very part of the tree where wood quality needs to be improved. Here too, the ability to characterise younger trees means that the rate of refinement can be increased.

But the laboratory is not only active in tree breeding. NIR technology is applicable in industrial processes, and the NIR camera can be used to create models for the prediction of physical and chemical properties. Examples of such properties include tree species, core/splinter, rot, moisture, lignin, cellulose, resin, minerals, etc. Examples of ongoing projects include the characterisation of wood chips for pulp production, timber in consideration measurement and identification of undesirable properties in furniture components.

In addition, the laboratory is also involved in product and process development projects, such as the evaluation of the results of impregnating wood with the NIR camera. Clearly, there are opportunities for the laboratory to contribute in more areas. It is the imagination that sets the limits for the laboratory's use. The challenge, however, is that potential customers are aware of their problems and how the laboratory's offer can contribute.

Further reading
High-resolution wood characterisation in laboratory environment

This is an article from our magazine Trävärden, view it here! (Link)

Biobased materials Sekundär områdes navigation:
Metrology
Agriculture
Chemical and biological analysis

Cement and different types of binders at RISE

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Cement and different types of binders Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

Our services for binder chemistry are consulting meetings, identification of new materials, reactivity tests, validation of SCM, regulation & standardization, the potential of new SCM, and characterization of alternative binders.

Purpose/Benefit:

Presently, Portland cement is the most important material used in concrete, and in enormous quantities, more than 4 billion tons globally. It is also a significant contributor to the total anthropogenic emissions of carbon dioxide, standing at 8% nowadays. There is a large interest in finding new sources for potential materials that can be used in two different ways: binders and alternative binders. 

For the cement industry, a binder is an ordinary Portland cement (OPC) based material where a part of cement is substituted by supplementary cementitious materials (SCM). An SCM can be a natural material such as clay or a by-product from other industries such as fly ash or ground granulated blast furnace slag. The substitution of cement by SCM can be between 5 and 65%. The replacement by SCM leads to a reduction of the CO2 emission link to cement production as less OPC is used.

An alternative binder is a material that has similar properties that ordinary Portland cement (OPC) but does not contain any OPC. They are becoming increasingly important for the transition to climate climate-neutral construction industry. There is a need to develop new alternative binders with low CO2 -footprint.

RISE has expertise in the entire binder value chain starting from chemical analyses to large-scale structural implementation. 

Method (what/which methods are used to perform the service):

If you are interested in the development, testing, and evaluation of any potential material that can be used as an SCM or alternative binder, RISE can offer a consulting discussion before any testing starts. The services we offer are listed below:

•  Consulting meeting 

  • Talk to our experts at RISE if you think you have a resource that can be potentially used as supplementary cementitious materials SCM or alternative binder
  • Our experienced experts will propose a plan of action by validating your ideas, understanding your perspective, and theoretically evaluating the actual potential

• Our general services include:

  • Identification of new material sources for the production of SCM or alternative binders
  • Testing the reactivity in cement
  • Validation testing of SCMs in concrete applications
  • Possibilities according to the regulation and standardization for the introduction of new materials in concrete in Sweden (link to a description)

• Testing properties of conventional SCMs (fly ash (FA), granulated ground furnace slag (GGBS)): While GGBFS and FA have been used for decades, their properties need to be tested for new sources, applications, markets, and conditions. Approach us for testing and analysis if you have:

  • New sources of conventional SCMs
  • New applications of conventional SCMs
  • Introduce your SCMs in new markets

• Assessment of potential new SCMs (high-volume materials rich in Al2O3, SiO2, Ca, Mg, Fe, etc.): Availability of conventional SCMs is decreasing as we move to greener sources of energy production (thereby reducing coal FA) and ferrous metal production (thereby reducing conventional GGBFS). There is a push to develop new SCMs, even if at additional cost of production and development.

  • Approach us for testing and analysis if you have high-volume materials rich in Al2O3, SiO2, CaO, MgO, Fe2O3, etc. Examples of such products are:
    • Calcined clay
    • Metallurgical industry wastes
    • Mining wastes
    • Incineration ashes
    • Paper/Pulp production wastes
    • Dredging sediments
  • In addition to test reactivity, we develop activation methods for different selected materials to be used as SCM. Some materials cannot be used as it is. A pre-treatment such as calcination, grinding, washing, …  is necessary to enhance the properties of the materials

• Characteriztion of alternative binders: RISE can provide materials characterization and property testing of alternative binders ie. calcium sulfoaluminate cement (CSA), Belite-Ye'elimite-Ferrite Cement, prehydrated calcium silicate cement, magnesium silicate cement, etc.

  • Composition and particle size analysis by micro-XRF, XRD, and particle analyzer
  • Heat of hydration by isothermal calorimetry
  • Setting time and strength testing 
  • Durability testing such as testing for shrinkage/expansion, resistance to freeze-thaw cycles, chloride ion penetration, and sulfate attack
  • Compatibility testing with other binders, SCMs, and additives

Welcome to contact us if you want to know more about what RISE does in cement, SCM, and alternative binders. 

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Consulting services and reports from testing

Area: Cement and concrete Contact person (Enter one name per field. Activated personal contact pages will appear automatically):
Gilles Plusquellec, Forskare
Yiru Yan, Forskare
Binder chemistry
Field measurements: No Price type: 1 Division: Do not use - Division Built Environment Preparation: No preparation required Certification and marking: Not applicable Type of service: Testing / Analysis / Evaluation Instrument: Not applicable General area: Not applicable Order information: Mer information Divison (OLD): Do not use - Division Built Environment Delivery level: Not applicable
gilles.plusquellec@ri.se,yiru.yan@ri.se
/en/node/9710
More information:

Potential new materials

  • Testing/validation of new materials such as calcined clays, metallurgical wastes, mining wastes, incineration ashes, pulp/paper industry wastes, dredging sediments, etc.
  • Extraction of valuable resources (critical, high value metals, etc.)

Characterization of SCMs to determine if it can be a good potential

  • Mineral phase identification
  • Micro-XRF for elemental quantification and mapping
  • Specific surface area, and particle size distribution
  • Thermal behavior using TGA/DSC

Activation of new SCMs 
(CO2, chemical, thermal, mechanical, etc.) 

  • CO2-mineralization as activation method
  • Controlled thermal activation
  • Mechanical activation to increase reactivity
  • Acid/chemical activation

Evaluation of the SCM reactivity in a cement matrix 

  • Bulk reactivity tests (R3, isothermal calorimetry, portlandite consumption, etc.)
  • SCM reaction and mechanisms: development of application methods accordingly
  • Particle-level hydration behavior
  • Activity index on mortar
  • Mechanical properties on mortar (compressive strength)

Validation testing of SCMs in concrete

  • Validation of SCMs for different regulatory cement types (CEM II, CEM III, etc.)
  • Concrete mix design development with SCM-cement.
  • Testing them according to desired exposure class
  • Concrete mechanical, durability, and environmental properties

Characterization and testing of Alternative binders

  • Materials characterizations (XRD, micro XRF, TGA, Particle size analyzer)
  • Reactions of alternative binders (hydration)
  • Properties of alternative binders (compressive strength, setting time, shrinkage-expansion, etc. 
  • Durability (carbonation, resistance to freeze-thaw, chloride peneration, sulfate attack)
  • Compatibility testing with other binders, SCM and additives

Regulatory/Market assistance

  • Assistance in identifying regulatory and compliance requirements for new SCM
  • Regulatory assistance for introduction of new SCMs in Swedish market, including testing and validation
  • Developing new industry collaborations

 

Our analysis are:

  • Micro-XRF
  • X-Ray Diffraction
  • Reactivity test
  • Cement hydration
  • Rheology
  • Compressive strength on mortar
Metod - Header: Our services More information - Header: More information
Order
form
Concrete and cement Sekundär områdes navigation:
Chemical and biological analysis
Materials and durability
Tjänstetyp tagg:
Konsultuppdrag
Provning

Analysis of Wood Extractives

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Analysis of Wood Extractives Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

Extractives are low molecular weight compounds that can be extracted from wood. The substances protect the tree against rot, pests and other attacks but can cause problems in industrial processes.

Purpose/Benefit:

Wood extractives are well-known to cause problems in the production process e.g. by formation of deposits on process equipment or foaming. The extractives may also give rise to spots in the pulp or paper, as well as negatively influence several paper properties. Isolated and modified wood extractives are also compounds with a very high added value in various fields as biochemicals (e.g., pharmaceuticals and cosmetics).

What can we do?

RISE has very long experience in analysis of wood extractives. We can offer a wide range of extraction and characterization techniques which, in combination, offer a detailed characterization of the extractives in various types of samples, for example:

• Extractive content (gravimetric) in all types of samples.  

• Chemical composition and quantification of Extractives in wood and bark, extractives in pulp and paper, tall oil in black liquor and Extractives in liquors and filtrates.  

• Characterization of deposits and spots.  

• Molecular weight distribution of extracts.  

Method (what/which methods are used to perform the service):

Extracts are derivatized and analyzed by GC/MS: Typically, individual fatty acids, resin acids, sterols, fatty alcohols, hydroxy acids etc. are quantified.  

Molecular mass distribution: The molecular mass of an extract is determined by size-exclusion chromatography (SEC), THF (tetrahydrofuran) or water-based systems. Detection with ultraviolet detector and/or refractive index detector and/or light scattering detector (MALS). 

Analysis with LC/MS: Water soluble compounds can be investigated and quantified by liquid chromatography combined with mass spectrometer. 

Phenolic groups: Sum of phenolic groups are determined using the Folin-Cocialteau spectrophotometric method. 

Characterization of extracts with Pyrolysis-GC/MS: The results are given in the form of chromatograms (pyrograms) with identification of seen compounds e.g. lignin, carbohydrates, tannins, extractives etc. Semi quantitative analysis. Very small samples (about 1 mg) can be analysed. 

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Results are compiled in an analysis report.

Area: Bioeconomy Contact person (Enter one name per field. Activated personal contact pages will appear automatically): Anders Reimann
Wood
Field measurements: No Price type: 1 Division: Division Bioeconomy Preparation: No preparation required Certification and marking: Not applicable Type of service: Not applicable Instrument: Not applicable General area: Not applicable Divison (OLD): Division Bioeconomy Delivery level: Not applicable
anders.reimann@ri.se
/en/node/10120
Purpose - Header: Wood extractives Metod - Header: Methods, Intrumentation and Expertise Delivery - Header: Delivery More information - Header: Mer information
Request for quote
form
Pulp and paper Sekundär områdes navigation:
Wood technology
Biobased materials
Chemical and biological analysis
Tjänstetyp tagg: Provning

Measuring the Molecular Weight Distribution of Lignin

Name of service (page headline, shown in promos – maximum of 70 characters incl. spaces): Measuring the Molecular Weight Distribution of Lignin Lead (include SEO-words and the main benefits for your target groups. Stick to one paragraph, maximum 2-3 sentences):

Molar mass and molar mass distribution is a fundamental property of lignin and an important characteristic for understanding and predicting polymer performance. We have equipment specialized for measuring molar mass distribution on lignin. 

Purpose/Benefit:

Knowing the molar mass distribution (MMD) is important to, for example, follow how the lignin is affected by different modifications and processes and to understand in which application a certain type of lignin would fit.  

Method (what/which methods are used to perform the service):

RISE has one THF-based SEC-system equipped with an RI and UV detector and one alkali-based SEC-system with three detectors, RI, UV and MALS (Multi-Angle Light Scattering), especially designed for lignin analysis.  

The lignin molecules are separated in a column based on their size. For the RI- and UV-detectors, the sample is compared to standards with known molecular weight, similar in structure to the lignin, to calculate the molecular weight of the sample. With the MALS-detector, light scattering is used to determine molecular weight, why calibration standards are not necessary. Hence, MALS gives the a direct estimation of the molecular weight. 

Delivery (what does the client get after performed service – e.g. a report, certificate etc.):

Results are compiled in an analysis report. 

Area: Bioeconomy Contact person (Enter one name per field. Activated personal contact pages will appear automatically): Sofia Regnell Andersson, Forskare
SEC
Field measurements: No Price type: 1 Division: Division Bioeconomy Preparation: Description of preparation Preparation information:

The customer is responsible for the preparation and transport of the test items.

Certification and marking: Not applicable Type of service: Not applicable Instrument: Not applicable General area: Not applicable Divison (OLD): Division Bioeconomy Delivery level: Non-accredited
sofia.regnell.andersson@ri.se
/en/node/9710
Purpose - Header: Purpose Metod - Header: Method Delivery - Header: Delivery More information - Header: More information
Request for quote
form
Chemical and biological analysis Sekundär områdes navigation:
Metrology
Biobased materials
Formulated products
Tjänstetyp tagg: Provning